2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

Base Information

Chemical Name:2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide
CAS No.:1583258-81-4
Molecular Formula:C₁₇H₁₀Br₂F₉NO₃S
Molecular Weight:639.131
Hs Code.:

Synonyms:2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

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Chemical Property of 2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

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Technology Process of 2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

There total 2 articles about 2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 6226-25-1
2,2,2-trifluoroethyl trifluoromethanesulphonate

: 1583258-79-0
2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)benzenesulfonamide

: 1583258-81-4
2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

Guidance literature:: With potassium carbonate; In acetonitrile; for 16h; Reflux;
DOI:10.1002/jlcr.3138

Reference yield:

: 722-92-9
2-(4-aminophenyl)-1,1,1,3,3,3-hexafluoro-2-propanol

: 1583258-81-4
2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / acetone / 36 h / Reflux

2: potassium carbonate / acetonitrile / 16 h / Reflux

With 2,6-dimethylpyridine; potassium carbonate; In acetone; acetonitrile;
DOI:10.1002/jlcr.3138

Reference yield:

: 1583258-81-4
2,4-dibromo-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

: 1583258-78-9
2,4-ditritium-N-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl)-N-(2,2,2-trifluoroethyl)benzenesulfonamide

Guidance literature:: With tritium; palladium 10% on activated carbon; potassium hydroxide; In methanol; at 23 ℃; for 3h; under 760.051 Torr;
DOI:10.1002/jlcr.3138