N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone

Base Information

Chemical Name:N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone
CAS No.:87674-02-0
Molecular Formula:C₂₆H₂₄ClN₅O₆
Molecular Weight:537.959
Hs Code.:

Synonyms:N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone

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Chemical Property of N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone

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Technology Process of N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone

There total 3 articles about N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 622-58-2,374675-64-6
p-Tolylisocyanate

: 61532-09-0
N-(1-hydroxy-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl)-4-nitrophenylnitrone

: 87674-02-0
N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -30 ℃;
DOI:10.1007/BF00516460

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 87674-02-0
N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ethanol / 0.5 h / Heating; standing overnight at r.t.

2: 89 percent / potassium tert-butoxide / tetrahydrofuran / -30 °C

With potassium tert-butylate; In tetrahydrofuran; ethanol;
DOI:10.1007/BF00516460

Reference yield:

: 56369-00-7
1-hydroxy-3-(3'-chlorophenyl)-5,5-dimethyl-4-hydroxylaminoimidazolidin-2-one

: 87674-02-0
N-<1-(4-tolylcarbamoyloxy)-3-(3-chlorophenyl)-5,5-dimethylimidazolidin-2-on-4-yl>-4-nitrophenylnitrone

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ethanol / 0.5 h / Heating; standing overnight at r.t.

2: 89 percent / potassium tert-butoxide / tetrahydrofuran / -30 °C

With potassium tert-butylate; In tetrahydrofuran; ethanol;
DOI:10.1007/BF00516460