Technology Process of C2HF3O2*C16H15N5O8S2
There total 4 articles about C2HF3O2*C16H15N5O8S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methyl-phenyl-thioether;
In
dichloromethane;
at 0 ℃;
for 18h;
DOI:10.1002/asia.201100647
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C
1.2: 30 h / 0 - 20 °C
2.1: methyl-phenyl-thioether / dichloromethane / 18 h / 0 °C
With
methyl-phenyl-thioether; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/asia.201100647
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 4-methyl-morpholine; triethylamine / dichloromethane / 4 h / 0 °C
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C
2.2: 30 h / 0 - 20 °C
3.1: methyl-phenyl-thioether / dichloromethane / 18 h / 0 °C
With
4-methyl-morpholine; methyl-phenyl-thioether; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/asia.201100647