(3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester

Base Information

Chemical Name:(3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester
CAS No.:615553-57-6
Molecular Formula:C₁₁H₁₀F₃NO₄
Molecular Weight:277.2
Hs Code.:

Synonyms:(3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester

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Chemical Property of (3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester

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Technology Process of (3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester

There total 1 articles about (3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 407-25-0
trifluoroacetic anhydride

: amino-(3-hydroxy-phenyl)-acetic acid methyl ester; hydrochloride

: 615553-57-6
(3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester

Guidance literature:: With TEA; In dichloromethane; for 4h;
DOI:10.1002/ejoc.200300044

Reference yield: 100.0%

: 615553-57-6
(3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester

: 615553-58-7
(3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid

Guidance literature:: With lithium hydroxide; In water; tert-butyl alcohol; at 20 ℃; for 1.66667h;
DOI:10.1002/ejoc.200300044

Reference yield:

: 615553-57-6
(3-hydroxy-phenyl)-(2,2,2-trifluoro-acetylamino)-acetic acid methyl ester

: 81017-73-4
(R)-Amino-(3-hydroxy-phenyl)-acetic acid; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / LiOH*H₂O / 2-methyl-propan-2-ol; H₂O / 1.67 h / 20 °C

2: acylase AMANO 30000; CoCl₂*6H₂O; NaN₃ / aq. phosphate buffer / 120 h / 25 °C / pH 7

3: 100 percent / HCl / H₂O; acetic acid / 65 °C

With hydrogenchloride; lithium hydroxide; sodium azide; acylase AMANO 30000; cobalt(II) chloride; In phosphate buffer; water; acetic acid; tert-butyl alcohol;
DOI:10.1002/ejoc.200300044