3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

Base Information

Chemical Name:3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester
CAS No.:499154-46-0
Molecular Formula:C₂₆H₃₅NO₅
Molecular Weight:441.568
Hs Code.:

Synonyms:3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

Suppliers and Price of 3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

There total 9 articles about 3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 499157-69-6
5-(methoxymethoxy)-2-(3-methoxy-3-oxopropyl)benzoic acid

: 499157-72-1
1-(3,5-dimethylphenyl)-3-methylbutan-1-amine hydrochloride

: 499154-46-0
3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 3h;

Reference yield:

: 72399-25-8
3-methylbutyraldehyde O-benzyl-oxime

: 499154-46-0
3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

1.2: 3 h

2.1: hydrogen / palladium 10% on activated carbon / methanol

3.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 3 h / 20 °C

With 4-methyl-morpholine; n-butyllithium; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide);

Reference yield:

: 93-35-6
7-hydroxy-2H-chromen-2-one

: 499154-46-0
3-(2-((3-methyl-1-(3,5-dimethylphenyl)butyl)carbamoyl)-4-methoxymethoxyphenyl)propanoic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-isopropylethylamine / DMF (N,N-dimethyl-formamide) / 4 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; methanol / 0.33 h / 20 °C

2.2: 0.67 h / 60 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 7 h / 20 °C

4.1: pyridine / dichloromethane / 0.17 h / 0 °C

5.1: potassium acetate; palladium diacetate / 1,1'-bis(diphenylphosphino)ferrocene / DMF (N,N-dimethyl-formamide) / 48 h / 90 °C

6.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 3 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogen; potassium acetate; palladium diacetate; sodium hydride; benzotriazol-1-ol; N-isopropylethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1,1'-bis(diphenylphosphino)ferrocene; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); dichloromethane;