2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione

Base Information

Chemical Name:2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione
CAS No.:657402-08-9
Molecular Formula:C₂₇H₃₄O₄
Molecular Weight:422.565
Hs Code.:

Synonyms:2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione

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Chemical Property of 2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione

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Technology Process of 2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione

There total 8 articles about 2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28752-82-1
2-(allyloxy)benzaldehyde

: 657402-08-9
2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 1.5 h / 0 - 25 °C

2: PCC / CH₂Cl₂ / 7 h / 40 °C

3: Et₃N / tetrahydrofuran / 12 h / 25 °C

4: diethyl ether / 1 h / 0 °C

With triethylamine; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ol036156w

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 657402-08-9
2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / acetone / 2 h / 56 °C

2: toluene / 1.5 h / 0 - 25 °C

3: PCC / CH₂Cl₂ / 7 h / 40 °C

4: Et₃N / tetrahydrofuran / 12 h / 25 °C

5: diethyl ether / 1 h / 0 °C

With potassium carbonate; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene;
DOI:10.1021/ol036156w

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 657402-08-9
2-[1-(2-Allyloxy-phenyl)-1-methoxy-meth-(E)-ylidene]-4,4-bis-(3-methyl-but-2-enyl)-cyclohexane-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / tetrahydrofuran / 12 h / 25 °C

2: diethyl ether / 1 h / 0 °C

With triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ol036156w