C₁₆H₁₀O₄S

Base Information

Chemical Name:C₁₆H₁₀O₄S
CAS No.:1369964-76-0
Molecular Formula:C₁₆H₁₀O₄S
Molecular Weight:298.319
Hs Code.:

C<sub>16</sub>H<sub>10</sub>O<sub>4</sub>S

Synonyms:C₁₆H₁₀O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₀O₄S

Chemical Property:

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Technology Process of C₁₆H₁₀O₄S

There total 5 articles about C₁₆H₁₀O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1345691-05-5
4-oxo-3-phenyl-4H-thiochromene-2-carbaldehyde

: 1369964-76-0
C₁₆H₁₀O₄S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid;
DOI:10.1016/j.tetlet.2016.09.065

Reference yield:

: 20848-85-5
2-methyl-3-phenyl-4H-thiochromen-4-one

: 1369964-76-0
C₁₆H₁₀O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: selenium(IV) oxide / 1,2-dichloro-benzene / 150 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C / Inert atmosphere

With selenium(IV) oxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1,2-dichloro-benzene;
DOI:10.1055/s-0031-1290326

Reference yield:

: 771-40-4
2-methyl-4H-thiochromen-4-one

: 1369964-76-0
C₁₆H₁₀O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium cerium (IV) nitrate; iodine / acetonitrile / 60 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

3: selenium(IV) oxide / 1,2-dichloro-benzene / 150 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C / Inert atmosphere

With selenium(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; ammonium cerium (IV) nitrate; iodine; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetonitrile; 2: Suzuki coupling;
DOI:10.1055/s-0031-1290326