Technology Process of C25H32O5
There total 12 articles about C25H32O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
camphor-10-sulfonic acid;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-BuLi / tetrahydrofuran / -18 °C
1.2: 97 percent / tetrahydrofuran / -18 °C
2.1: 96 percent / i-Pr2NEt / CH2Cl2 / Heating
3.1: methyl iodide; water / acetonitrile / 50 °C
3.2: NaBH4; CeCl3*7H2O / various solvent(s) / 0 °C
4.1: NaH / dimethylformamide / 0 °C
5.1: 76 percent / CSA / methanol
With
n-butyllithium; camphor-10-sulfonic acid; water; sodium hydride; N-ethyl-N,N-diisopropylamine; methyl iodide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 96 percent / i-Pr2NEt / CH2Cl2 / Heating
2.1: methyl iodide; water / acetonitrile / 50 °C
2.2: NaBH4; CeCl3*7H2O / various solvent(s) / 0 °C
3.1: NaH / dimethylformamide / 0 °C
4.1: 76 percent / CSA / methanol
With
camphor-10-sulfonic acid; water; sodium hydride; N-ethyl-N,N-diisopropylamine; methyl iodide;
In
methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;