C₄₇H₇₃BrO₁₀Si₂

Base Information

Chemical Name:C₄₇H₇₃BrO₁₀Si₂
CAS No.:1338566-25-8
Molecular Formula:C₄₇H₇₃BrO₁₀Si₂
Molecular Weight:934.166
Hs Code.:

C<sub>47</sub>H<sub>73</sub>BrO<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₇H₇₃BrO₁₀Si₂

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Chemical Property of C₄₇H₇₃BrO₁₀Si₂

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Technology Process of C₄₇H₇₃BrO₁₀Si₂

There total 4 articles about C₄₇H₇₃BrO₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338566-24-7
C₅₃H₇₈O₁₂SSi₂

: 1338566-25-8
C₄₇H₇₃BrO₁₀Si₂

Guidance literature:: With diethyl ether; lithium bromide; In dichloromethane; at 0 - 20 ℃; for 7h;
DOI:10.1021/ol202467z

Reference yield:

: 1338566-17-8
3-((2S,3R,4aS,6R,7S,8aR)-7-(benzyloxy)-6-((benzyloxy)methyl)-3-(t-butyldimethylsiloxy)octahydropyrano[3,2-b]pyran-2-yl)-1,2-epoxypropan-1-yl phenyl sulfone

: 1338566-25-8
C₄₇H₇₃BrO₁₀Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol; dichloromethane / 2 h / 0 °C

3: diethyl ether; lithium bromide / dichloromethane / 7 h / 0 - 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diethyl ether; toluene-4-sulfonic acid; lithium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol202467z

Reference yield:

: 1338566-18-9
C₂₂H₄₃F₃O₇SSi₂

: 1338566-25-8
C₄₇H₇₃BrO₁₀Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol; dichloromethane / 2 h / 0 °C

3: diethyl ether; lithium bromide / dichloromethane / 7 h / 0 - 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diethyl ether; toluene-4-sulfonic acid; lithium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol202467z