C₃₄H₄₃FN₂O₅

Base Information

Chemical Name:C₃₄H₄₃FN₂O₅
CAS No.:950524-67-1
Molecular Formula:C₃₄H₄₃FN₂O₅
Molecular Weight:578.724
Hs Code.:

C<sub>34</sub>H<sub>43</sub>FN<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₄H₄₃FN₂O₅

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Chemical Property of C₃₄H₄₃FN₂O₅

Chemical Property:

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Technology Process of C₃₄H₄₃FN₂O₅

There total 14 articles about C₃₄H₄₃FN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 950524-65-9
C₃₄H₄₁FN₂O₅

: 950524-67-1
C₃₄H₄₃FN₂O₅

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃; for 6h;
DOI:10.1016/j.bmcl.2007.05.097

Reference yield:

: 950524-22-8
C₁₂H₁₄FNO₃

: 950524-67-1
C₃₄H₄₃FN₂O₅

Guidance literature:: Multi-step reaction with 12 steps

1: 84 percent / trifluoroacetic anhydride; triethylamine / CH₂Cl₂ / 0.5 h / -10 °C

2: 92 percent / DBU / tetrahydrofuran / 18 h / 25 °C

3: 75 percent / KOH / dimethylsulfoxide / 2 h / 25 °C

4: 52 percent / NaIO₄; OsO₄ / tetrahydrofuran; H₂O / 18 h / 0 - 25 °C

5: 79 percent / Na(OAc)3BH; AcOH / 1,2-dichloro-ethane / 18 h / 25 °C

6: 94 percent / trimethylaluminum; triethylamine / CH₂Cl₂; toluene / 16 h / 60 °C

7: 97 percent / POCl₃ / 1,2-dichloro-ethane / 18 h / 80 °C

8: 56 percent / LiAl(O-t-Bu)3H / tetrahydrofuran / 0.5 h / 0 °C

9: 100 percent / CH₂Cl₂ / 2 h / 50 °C

10: 85 percent / NHMDS / tetrahydrofuran / 1 h / -78 - 25 °C

11: 84 percent / HCl / methanol / 2 h / 25 °C

12: 72 percent / H₂ / Pd/C / methanol / 6 h / 25 °C

With hydrogenchloride; potassium hydroxide; sodium periodate; osmium(VIII) oxide; hydrogen; trimethylaluminum; sodium hexamethyldisilazane; sodium tris(acetoxy)borohydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium tri-t-butoxyaluminum hydride; triethylamine; trifluoroacetic anhydride; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene; 7: Vilsmeier-Haack formylation / 10: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.097

Reference yield:

: 950524-28-4
C₂₅H₂₉FN₂O₂

: 950524-67-1
C₃₄H₄₃FN₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / trimethylaluminum; triethylamine / CH₂Cl₂; toluene / 16 h / 60 °C

2: 97 percent / POCl₃ / 1,2-dichloro-ethane / 18 h / 80 °C

3: 56 percent / LiAl(O-t-Bu)3H / tetrahydrofuran / 0.5 h / 0 °C

4: 100 percent / CH₂Cl₂ / 2 h / 50 °C

5: 85 percent / NHMDS / tetrahydrofuran / 1 h / -78 - 25 °C

6: 84 percent / HCl / methanol / 2 h / 25 °C

7: 72 percent / H₂ / Pd/C / methanol / 6 h / 25 °C

With hydrogenchloride; hydrogen; trimethylaluminum; sodium hexamethyldisilazane; lithium tri-t-butoxyaluminum hydride; triethylamine; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane; toluene; 2: Vilsmeier-Haack formylation / 5: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.097