phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate

Base Information

Chemical Name:phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate
CAS No.:1228046-84-1
Molecular Formula:C₂₆H₂₁N₅O₃
Molecular Weight:451.484
Hs Code.:

Synonyms:phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate

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Chemical Property of phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate

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Technology Process of phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate

There total 2 articles about phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1228046-83-0
phenyl 2-(2-cyanoacetamido)-3-(1H-indol-3-yl)propanoate

: 62-53-3
aniline

: 1228046-84-1
phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate

Guidance literature:: aniline; With hydrogenchloride; sodium nitrite; Cooling;

phenyl 2-(2-cyanoacetamido)-3-(1H-indol-3-yl)propanoate; With sodium acetate; In ethanol; at 0 - 20 ℃;
DOI:10.1002/ardp.200900244

Reference yield:

: phenyl 2-amino-3-(1H-indol-3-yl)propanoate

: 1228046-84-1
phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 4 h / Reflux

2.1: hydrogenchloride; sodium nitrite / Cooling

2.2: 0 - 20 °C

With hydrogenchloride; sodium nitrite; In N,N-dimethyl-formamide;
DOI:10.1002/ardp.200900244

Reference yield:

: 1228046-84-1
phenyl 2-(2-cyano-2-phenylhydrazonoacetamido)-3-(1H-indol-3-yl)propanoate

: 1228046-88-5
6-[4-(1H-indol-3-yl)methyl-5-hydroxyoxazol-2-yl]-2,4-diphenyl-3-thioxo-1,2,4-triazin-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / Reflux

2: triethylamine / N,N-dimethyl-formamide / 4 h / Reflux

3: sodium hydroxide / ethanol / 3 h / Reflux

With acetic acid; triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/ardp.200900244