C₁₃H₁₁F₄N₃

Base Information

Chemical Name:C₁₃H₁₁F₄N₃
CAS No.:1383735-55-4
Molecular Formula:C₁₃H₁₁F₄N₃
Molecular Weight:285.244
Hs Code.:

C<sub>13</sub>H<sub>11</sub>F<sub>4</sub>N<sub>3</sub>

Synonyms:C₁₃H₁₁F₄N₃

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Chemical Property of C₁₃H₁₁F₄N₃

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Technology Process of C₁₃H₁₁F₄N₃

There total 6 articles about C₁₃H₁₁F₄N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383735-52-1
1-(4-fluorophenyl)-5-trifluoromethyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-b]pyridine

: 1383735-56-5
C₁₃H₁₁F₄N₃

: 1383735-55-4
C₁₃H₁₁F₄N₃

Guidance literature:: With AD column; In n-heptane; isopropyl alcohol; Resolution of racemate;

Reference yield:

: 352-34-1
4-fluoro-1-iodobenzene

: 1383735-56-5
C₁₃H₁₁F₄N₃

: 1383735-55-4
C₁₃H₁₁F₄N₃

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / N,N-dimethyl-formamide / 1.5 h / 140 °C / microwave irradiation

2: hydrogenchloride; hydrogen / palladium 10% on activated carbon / 1,4-dioxane; methanol / 3 h / 50 °C / 15514.9 - 18100.7 Torr

3: AD column / isopropyl alcohol; n-heptane / Resolution of racemate

With hydrogenchloride; hydrogen; potassium carbonate; copper(l) iodide; palladium 10% on activated carbon; cis-N,N'-dimethyl-1,2-diaminocyclohexane; In 1,4-dioxane; methanol; n-heptane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 383907-17-3
2-methyl-6-(trifluoromethyl)pyridin-3-amine

: 1383735-56-5
C₁₃H₁₁F₄N₃

: 1383735-55-4
C₁₃H₁₁F₄N₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 144 h

2.1: acetic anhydride; potassium acetate; acetic acid; isopentyl nitrite / toluene / 1 h / Reflux

2.2: 1 h / Reflux

3.1: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / N,N-dimethyl-formamide / 1.5 h / 140 °C / microwave irradiation

4.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / 1,4-dioxane; methanol / 3 h / 50 °C / 15514.9 - 18100.7 Torr

5.1: AD column / isopropyl alcohol; n-heptane / Resolution of racemate

With hydrogenchloride; hydrogen; potassium acetate; acetic anhydride; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; isopentyl nitrite; dmap; copper(l) iodide; palladium 10% on activated carbon; cis-N,N'-dimethyl-1,2-diaminocyclohexane; In 1,4-dioxane; methanol; n-heptane; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene;