2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate

Base Information

Chemical Name:2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate
CAS No.:126377-47-7
Molecular Formula:C₂₁H₃₁N₃O₂Si
Molecular Weight:385.582
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate

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Technology Process of 2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate

There total 3 articles about 2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30290-07-4
4⁽⁵⁾-(2-bromoethyl)imidazole hydrobromide

: 126377-47-7
2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium ethoxide / 1.) ethanol, 10 min, 2.) RT, 6 h

2: 74 percent / water / 168 h / Heating

3: 1.) triethylamine, diphenyl phosphorazidate (DPPA) / 1.) toluene, 80 deg C, 2 h, 2.) 80 deg C, 22 h

With diphenyl phosphoryl azide; water; sodium ethanolate; triethylamine;
DOI:10.1021/jm00168a024

Reference yield:

: 126377-45-5
diethyl 2-<(1H-imidazol-4-yl)ethyl>-2-(3-phenyl-2-trans-propenyl)propanedioate

: 126377-47-7
2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / water / 168 h / Heating

2: 1.) triethylamine, diphenyl phosphorazidate (DPPA) / 1.) toluene, 80 deg C, 2 h, 2.) 80 deg C, 22 h

With diphenyl phosphoryl azide; water; triethylamine;
DOI:10.1021/jm00168a024

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 126377-46-6
α-(3-phenyl-2-trans-propenyl)-1H-imidazole-4-butanoic acid

: 126377-47-7
2-(trimethylsilyl)ethyl <1-<2-(1H-imidazol-4-yl)ethyl>-4-phenyl-3-trans-butenyl>carbamate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; Yield given. Multistep reaction; 1.) toluene, 80 deg C, 2 h, 2.) 80 deg C, 22 h;
DOI:10.1021/jm00168a024