C₂₅H₃₄O₆

Base Information

Chemical Name:C₂₅H₃₄O₆
CAS No.:391278-07-2
Molecular Formula:C₂₅H₃₄O₆
Molecular Weight:430.541
Hs Code.:

C<sub>25</sub>H<sub>34</sub>O<sub>6</sub>

Synonyms:C₂₅H₃₄O₆

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Chemical Property of C₂₅H₃₄O₆

Chemical Property:

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Technology Process of C₂₅H₃₄O₆

There total 23 articles about C₂₅H₃₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 391278-06-1
C₂₆H₃₈O₉S

: 391278-07-2
C₂₅H₃₄O₆

Guidance literature:: With sodium hydride; In tetrahydrofuran; Heating;
DOI:10.1016/S0040-4039(01)01802-0

Reference yield: 83.0%

: 391278-05-0
C₂₅H₃₆O₇

: 391278-07-2
C₂₅H₃₄O₆

Guidance literature:: C₂₅H₃₆O₇; With 2,4,6-trimethyl-pyridine; methanesulfonyl chloride; In dichloromethane; at 0 ℃; for 48h;

With sodium hydride; In tetrahydrofuran; for 4h; Heating;
DOI:10.1016/j.tet.2004.07.094

Reference yield:

: 391277-96-6
C₁₆H₂₆O₅

: 391278-07-2
C₂₅H₃₄O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: 93 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / 20 °C

2.1: 92 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

3.1: K₂CO₃ / methanol / 4 h / 20 °C

3.2: 90 percent / PCC / CH₂Cl₂ / 3 h / 20 °C

4.1: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

5.1: 73 percent / Na₂(EDTA); oxone; NaHCO₃ / H₂O; acetone; acetonitrile / 4 h / 20 °C

6.1: 79 percent / Al(OiPr)3 / toluene / 1 h / 20 °C

7.1: Me₃SiCl; Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 20 °C

7.2: tetrahydrofuran / 0.17 h / -78 °C

7.3: 90 percent / HCl / tetrahydrofuran; H₂O / 0.5 h / 20 °C

8.1: NaH / tetrahydrofuran / 0 - 20 °C

8.2: 86 percent / tetrahydrofuran / 12 h / Heating

9.1: OsO₄; N-methylmorpholine-N-oxide / acetone; H₂O / 96 h / 20 °C

9.2: 78 percent / NaIO₄ / acetone; H₂O / 48 h / 20 °C

10.1: 70 percent / H₂ / Pd/C / ethyl acetate

11.1: 100 percent / NaBH₄ / methanol / 0.5 h / 0 °C

12.1: 2,4,6-collidine; MsCl / CH₂Cl₂ / 48 h / 0 °C

12.2: 83 percent / NaH / tetrahydrofuran / 4 h / Heating

With 2,4,6-trimethyl-pyridine; dmap; Oxone; sodium tetrahydroborate; osmium(VIII) oxide; chloro-trimethyl-silane; hydrogen; edetate disodium; aluminum isopropoxide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; methanesulfonyl chloride; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; 1.1: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2004.07.094