3,4-dimethyl-1-phenylphospholane oxide

Base Information

Chemical Name:3,4-dimethyl-1-phenylphospholane oxide
CAS No.:46244-10-4
Molecular Formula:C₁₂H₁₇OP
Molecular Weight:208.24
Hs Code.:

Synonyms:3,4-dimethyl-1-phenylphospholane oxide

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Chemical Property of 3,4-dimethyl-1-phenylphospholane oxide

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Technology Process of 3,4-dimethyl-1-phenylphospholane oxide

There total 1 articles about 3,4-dimethyl-1-phenylphospholane oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 710-89-4
3,4-dimethyl-1-phenyl-3-phospholene 1-oxide

: 46244-10-4
3,4-dimethyl-1-phenylphospholane oxide

Guidance literature:: With 10% palladium on activated charcoal; hydrogen; In methanol; at 60 ℃; under 9375.94 Torr;
DOI:10.1002/hc.20579

Reference yield:

: 46244-10-4
3,4-dimethyl-1-phenylphospholane oxide

: 36071-31-5
C₁₂H₁₇P

Guidance literature:: With pyridine; trichlorosilane; In toluene; at 110 ℃; for 2h; Inert atmosphere;
DOI:10.1002/hc.20579

Reference yield:

: 46244-10-4
3,4-dimethyl-1-phenylphospholane oxide

: C₁₂H₂₀BP

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; trichlorosilane / toluene / 2 h / 110 °C / Inert atmosphere

2: dimethylsulfide borane complex / toluene / 24 h / 26 °C / Inert atmosphere

With pyridine; dimethylsulfide borane complex; trichlorosilane; In toluene;
DOI:10.1002/hc.20579