2,4-Dimethoxyacetophenone Hydrazone

Base Information

• Chemical Name: 2,4-Dimethoxyacetophenone Hydrazone
• CAS No.: 77336-34-6
• Molecular Formula: C₁₀H₁₄N₂O₂
• Molecular Weight: 194.233
• Mol file: 77336-34-6.mol

Synonyms:2,4-Dimethoxyacetophenone Hydrazone

Chemical Property of 2,4-Dimethoxyacetophenone Hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2,4-Dimethoxyacetophenone Hydrazone

There total 1 articles about 2,4-Dimethoxyacetophenone Hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2',4'-dimethoxyacetophenone (829-20-9) → 2,4-Dimethoxyacetophenone Hydrazone (77336-34-6)

Guidance literature:

With boron trifluoride diethyl etherate; hydrazine; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1134/S1070363216120471

Reference yield:

2,4-Dimethoxyacetophenone Hydrazone (77336-34-6) → 1-(1-Iodo-vinyl)-2,4-dimethoxy-benzene (77336-35-7)

Guidance literature:

With iodine; triethylamine; In tetrahydrofuran; for 1h;

Reference yield:

2,4-Dimethoxyacetophenone Hydrazone (77336-34-6) → 1,3-dimethoxy-4-ethynylbenzene (77336-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: I₂, triethylamine / tetrahydrofuran / 1 h

2: 1.01 g / NaH / tetrahydrofuran / Heating

With iodine; sodium hydride; triethylamine; In tetrahydrofuran;

upstream raw materials:

2',4'-dimethoxyacetophenone

Downstream raw materials:

1-(1-Iodo-vinyl)-2,4-dimethoxy-benzene

1,3-dimethoxy-4-ethynylbenzene