(2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)

Base Information

Chemical Name:(2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)
CAS No.:1083419-76-4
Molecular Formula:C₄₀H₅₆N₂O₇
Molecular Weight:676.894
Hs Code.:

Synonyms:(2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)

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Chemical Property of (2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)

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Technology Process of (2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)

There total 1 articles about (2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33884-43-4
2-(2-Bromoethyl)-1,3-dioxane

: 1083419-74-2
C₄₈H₅₆N₂O₉

: 1083419-76-4
(2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)

Guidance literature:: 2-(2-Bromoethyl)-1,3-dioxane; With magnesium; In tetrahydrofuran;

C₄₈H₅₆N₂O₉; In tetrahydrofuran; at 60 ℃; for 72h;

With water; ammonium chloride; In tetrahydrofuran; at 20 ℃; diastereoselective reaction;
DOI:10.1021/jo801700f

Reference yield: 85.0%

: 1083419-76-4
(2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)

: 1083419-78-6
3-benzyloxy-1,3-bis[(2-hydroxy-1(R)-phenylethyl)pyrrolidin-2(S)-yl]propane

Guidance literature:: (2R,2'R)-2,2'-[5-benzyloxy-1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol); With hydrogenchloride; water; In methanol; for 3h; Reflux;

With sodium cyanoborohydride; In methanol; at 20 ℃; for 2.5h;
DOI:10.1021/jo801700f