bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide

Base Information

• Chemical Name: bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide
• CAS No.: 103867-55-6
• Molecular Formula: C₂₄H₃₂Br₂O₂
• Molecular Weight: 512.325
• Mol file: 103867-55-6.mol

Synonyms:bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide

Chemical Property of bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide

There total 3 articles about bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

2-<4-(1-methyl-2-bromoethyl)phenyl>-2-propanol (103867-53-4) + 2-<4-(1-methyl-2-bromoethyl)phenyl>-2-hydroperoxypropane (103867-54-5) → bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide (103867-55-6)

Guidance literature:

perchloric acid; In acetic acid; at 20 ℃; for 5h;

Reference yield:

1-(1-methyl-2-bromoethyl)-4-acetylbenzene (103867-52-3) → bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide (103867-55-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / diethyl ether / 1 h / 0 - 5 °C

2: 73 percent / perchloric acid / acetic acid / 5 h / 20 °C

perchloric acid; In diethyl ether; acetic acid;

Reference yield:

2-<4-(1-methyl-2-bromoethyl)phenyl>-2-propanol (103867-53-4) → bis<1-methyl-1-<4-(1-methyl-2-bromoethyl)phenyl>ethyl> peroxide (103867-55-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 59 percent / 30percent hydrogen peroxide, 94percent sulfuric acid / CHCl₃ / 3 h / 0 - 3 °C

2: 73 percent / perchloric acid / acetic acid / 5 h / 20 °C

With sulfuric acid; dihydrogen peroxide; perchloric acid; In chloroform; acetic acid;

upstream raw materials:

2-<4-(1-methyl-2-bromoethyl)phenyl>-2-propanol

2-<4-(1-methyl-2-bromoethyl)phenyl>-2-hydroperoxypropane

1-(1-methyl-2-bromoethyl)-4-acetylbenzene

Downstream raw materials:

bis<1-methyl-1-<4-(2-bromo-1-methyl-1-hydroxyethyl)phenyl>ethyl> peroxide

bis<1-methyl-1-(4-isopropenylphenyl)ethyl> peroxide