N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide

Base Information

• Chemical Name: N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide
• CAS No.: 405920-12-9
• Molecular Formula: C₃₁H₂₉NOS₃
• Molecular Weight: 527.775
• Mol file: 405920-12-9.mol

Synonyms:N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide

Chemical Property of N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide

There total 1 articles about N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

phenylmethanethiol (100-53-8) + N-(1-benzenesulfonyl-2,2-dichloro-vinyl)-4-methyl-benzamide → N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide (405920-12-9)

Guidance literature:

With triethylamine; In ethanol; at 20 - 25 ℃; for 2h; Electrolysis;

DOI:10.1023/A:1013196415680

Reference yield: 66.0%

N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide (405920-12-9) → 4,5-di(benzylthio)-2-p-tolyloxazole (405920-22-1)

Guidance literature:

With thionyl chloride; In benzene; for 1h; Heating;

DOI:10.1023/A:1013196415680

Reference yield:

N-[1,2,2-tri(benzylthio)ethenyl]-p-toluoylamide (405920-12-9) → 4,5-bis-phenylmethanesulfonyl-2-p-tolyl-oxazole

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / thionyl chloride / benzene / 1 h / Heating

2: 40 percent / acetic acid; hydrogen peroxide / H₂O / Heating

With thionyl chloride; dihydrogen peroxide; acetic acid; In water; benzene;

DOI:10.1023/A:1013196415680

upstream raw materials:

phenylmethanethiol

Downstream raw materials:

4,5-di(benzylthio)-2-p-tolyloxazole