1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid

Base Information

• Chemical Name: 1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid
• CAS No.: 912290-61-0
• Molecular Formula: C₁₇H₁₆N₂O₆S
• Molecular Weight: 376.39

Synonyms:1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid

Chemical Property of 1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid

Chemical Property:

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Technology Process of 1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid

There total 2 articles about 1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N-[(1-formylcyclopropyl)(phenyl)methyl]-4-nitrobenzenesulfonamide (912290-60-9) → 1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid (912290-61-0)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In water; acetone; at 20 ℃; for 72h;

DOI:10.1002/anie.200600961

Reference yield:

cis-4-benzyloxy-5-(4-nitrobenzenesulfonyl)-6-phenyl-5-azaspiro[2.3]hexane → 1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid (912290-61-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / Amberlyst-15 H⁽¹⁺⁾ / acetone; H₂O / 20 °C

2: 90 percent / CrO₃; H₂SO₄ / H₂O; acetone / 72 h / 20 °C

With chromium(VI) oxide; Amberlyst-15 H⁽¹⁺⁾; sulfuric acid; In water; acetone;

DOI:10.1002/anie.200600961

Reference yield: 100.0%

1-[(4-nitrobenzenesulfonylamino)(phenyl)methyl]cyclopropanecarboxylic acid (912290-61-0) → 1-[amino(phenyl)methyl]cyclopropanecarboxylic acid

Guidance literature:

With Amberlyst A-21; ethyl 2-sulfanylacetate; In acetonitrile; at 20 ℃; for 72h;

DOI:10.1002/anie.200600961

upstream raw materials:

N-[(1-formylcyclopropyl)(phenyl)methyl]-4-nitrobenzenesulfonamide

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