cis-{PdCl₂(PPh₃)(3IPA)

Base Information

• Chemical Name: cis-{PdCl₂(PPh₃)(3IPA)
• CAS No.: 120272-61-9
• Molecular Formula: C₂₅H₂₄Cl₂NO₂PPd
• Molecular Weight: 578.771

Synonyms:cis-{PdCl₂(PPh₃)(3IPA)

Chemical Property of cis-{PdCl₂(PPh₃)(3IPA)

Chemical Property:

Purity/Quality:

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Technology Process of cis-{PdCl₂(PPh₃)(3IPA)

There total 1 articles about cis-{PdCl₂(PPh₃)(3IPA) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3-isocyanopropyl acrylate + [PdCl2(triphenylphosphine)]2 → cis-{PdCl2(PPh3)(3IPA) (120272-61-9)

Guidance literature:

In benzene; addn. of 3IPA-soln. to suspension of Pd-complex at room temp. for 30 min. (N2), stirring for 30 min.; filtration, concn., pptn. with Et2O, recrystn. (activated carbon, CH2Cl2-Et2O);

DOI:10.1016/S0020-1693(00)83492-1

Reference yield:

cis-{PdCl2(PPh3)(3IPA) (120272-61-9) → palladium (7440-05-3)

Guidance literature:

With H₂; In tetrahydrofuran; stirring with H2 at room temp.in THF for 7 days;

DOI:10.1016/S0020-1693(00)80269-8

Reference yield:

ethyleneimine (151-56-4,9002-98-6) + cis-{PdCl2(PPh3)(3IPA) (120272-61-9) → PdCl2P(C6H5)3{C3H5N2(CH2)3OC(O)CHCH2}

Guidance literature:

In tetrahydrofuran; addn. of aziridine to soln. of Pd-complex at 0°C, allowing to warm to room temp. after 10 min., stirring overnight (pptn.); filtration, washing (n-hexane, crude yield 73%), washing (acetone and n-hexane), recrystn. (CH2Cl2-n-hexane);

DOI:10.1016/S0020-1693(00)83492-1

Downstream raw materials:

palladium

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