N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide

Base Information

Chemical Name:N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide
CAS No.:1159107-87-5
Molecular Formula:C₁₄H₁₄ClN₅O₃
Molecular Weight:335.75
Hs Code.:

Synonyms:N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide

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Chemical Property of N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide

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Technology Process of N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide

There total 2 articles about N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 541-88-8
Chloroacetic anhydride

: 4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidine-2,4-diamine

: 1159107-87-5
N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide

Guidance literature:: In tetrahydrofuran; at 0 - 23 ℃; for 1.5h;
DOI:10.1002/hlca.200900009

Reference yield: 71.0%

: 541-88-8
Chloroacetic anhydride

: 4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidine-2,4-diamine

: 1159107-89-7
2-amino-4-(benzyloxy)-6-chloro-8-methylpteridin-7(8H)-one

: 1159107-87-5
N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide

Guidance literature:: With dmap; In tetrahydrofuran; at 0 - 23 ℃; for 1.5h;
DOI:10.1002/hlca.200900009

Reference yield: 55.0%

: 1159107-87-5
N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide

: 1066-54-2
trimethylsilylacetylene

: 1159108-03-8
6,6'-(ethyne-1,2-diyl)bis[2-amino-4-(benzyloxy)-8-methylpteridin-7(8H)-one]

Guidance literature:: N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide; trimethylsilylacetylene; With copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine; In acetonitrile; at 23 ℃; for 7h;

With tetra-n-butylammoniumfluoride trihydrate; In acetonitrile; for 0.5h;

N-[4-(benzyloxy)-6-(methylamino)-5-nitrosopyrimidin-2-yl]-2-chloroacetamide; In acetonitrile;
DOI:10.1002/hlca.200900009