1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate

Base Information

Chemical Name:1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate
CAS No.:1137150-74-3
Molecular Formula:C₁₉H₂₄O₇
Molecular Weight:364.395
Hs Code.:

Synonyms:1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate

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Chemical Property of 1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate

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Technology Process of 1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate

There total 1 articles about 1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1137150-65-2
1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] (2S)-2-(2-methoxy-2-oxoethyl)oxirane-2-carboxylate

: 29917-94-0
2-methylprop-1-enyllithium

: 1137150-74-3
1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate

Guidance literature:: 2-methylprop-1-enyllithium; With copper(l) iodide; In diethyl ether; at -78 - -60 ℃; for 1.5h;

1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] (2S)-2-(2-methoxy-2-oxoethyl)oxirane-2-carboxylate; In diethyl ether; at -78 ℃; for 2h;
DOI:10.1002/ejoc.200800935

Reference yield: 76.0%

: 1137150-74-3
1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate

: 1137150-75-4
(1S)-2-methoxy-2-oxo-1-phenylethyl (2R)-2-(2-methoxy-2-oxoethyl)-5,5-dimethyltetrahydrofuran-2-carboxylate

Guidance literature:: 1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-hydroxy-2-(3-methylbut-2-en-1-yl)butanedioate; With mercury(II) acetate; In tetrahydrofuran; water; at 20 ℃; for 2.5h;

With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1002/ejoc.200800935