alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

Base Information

Chemical Name:alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide
CAS No.:106513-17-1
Molecular Formula:C₃₇H₅₉N₁₃O₁₃
Molecular Weight:893.955
Hs Code.:

Synonyms:alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

Suppliers and Price of alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

There total 7 articles about alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 111705-69-2
tert-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

: 106513-17-1
alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

Guidance literature:: With hydrogen; palladium; In water; acetic acid; for 2h; Ambient temperature;

Reference yield:

: 51342-92-8
L-asparginyl-L-phenylalanyl methyl ester

: 106513-17-1
alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

Guidance literature:: Multi-step reaction with 7 steps

1: 1) pivaloyl chloride, N-ethylpiperidine, pyridine / 1) dichloromethane, 8 min., 0 deg C; 2) 2 h, room temp.

2: 78 percent / liq. NH₃ / methanol; H₂O / 70 h / Ambient temperature

3: 96 percent / H₂ / Pd-black / acetic acid; methanol; H₂O / 3 h / Ambient temperature

4: 1) NaNO₂, N-ethylpiperidine ; 2) N-ethylpiperidine / 1) conc. HCl, DMF, 10 min., -20 deg C; 2) 12 h, 0 deg C

5: 86 percent / H₂ / Pd-black / dimethylformamide; methanol; acetic acid / 6 h / Ambient temperature

6: 1) 1-hydroxybenztriazole, N,N'-dicyclohexylcarbodiimide / 1) DMF, -10 deg C, 10 min.; 2) 2 h, 0 deg C, then 8 h, room temp.

7: 57 percent / H₂ / Pd-black / acetic acid; H₂O / 2 h / Ambient temperature

With 1-ethyl-piperidine; pyridine; ammonia; hydrogen; pivaloyl chloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; palladium; In methanol; water; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 106513-29-5
seryl-asparaginyl-phenylalanine amide

: 106513-17-1
alanyl-lysyl-seryl-glutaminyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine amide

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NaNO₂, N-ethylpiperidine ; 2) N-ethylpiperidine / 1) conc. HCl, DMF, 10 min., -20 deg C; 2) 12 h, 0 deg C

2: 86 percent / H₂ / Pd-black / dimethylformamide; methanol; acetic acid / 6 h / Ambient temperature

3: 1) 1-hydroxybenztriazole, N,N'-dicyclohexylcarbodiimide / 1) DMF, -10 deg C, 10 min.; 2) 2 h, 0 deg C, then 8 h, room temp.

4: 57 percent / H₂ / Pd-black / acetic acid; H₂O / 2 h / Ambient temperature

With 1-ethyl-piperidine; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; palladium; In methanol; water; acetic acid; N,N-dimethyl-formamide;