(4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

Base Information

Chemical Name:(4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane
CAS No.:516457-41-3
Molecular Formula:C₁₈H₂₈O₅S₂
Molecular Weight:388.549
Hs Code.:

Synonyms:(4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

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Chemical Property of (4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

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Technology Process of (4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

There total 3 articles about (4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 33577-16-1
methyl methylsulfinylmethyl sulfide

: 516457-86-6
(4R,5S)-4-Iodomethyl-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

: 516457-41-3
(4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/ol0341804

Reference yield:

: 118620-86-3,132437-17-3
(2S,3S)-4-(p-methoxybenzyloxy)-2,3-(isopropylidenedioxy)-butan-1-ol

: 516457-41-3
(4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: NaI; CaCO₃ / acetone

3: 87 percent / n-BuLi / tetrahydrofuran; hexane

With pyridine; n-butyllithium; calcium carbonate; sodium iodide; In tetrahydrofuran; hexane; acetone;
DOI:10.1021/ol0341804

Reference yield:

: Toluene-4-sulfonic acid (4S,5S)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 516457-41-3
(4S,5S)-4-(2-Methanesulfinyl-2-methylsulfanyl-ethyl)-5-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: NaI; CaCO₃ / acetone

2: 87 percent / n-BuLi / tetrahydrofuran; hexane

With n-butyllithium; calcium carbonate; sodium iodide; In tetrahydrofuran; hexane; acetone;
DOI:10.1021/ol0341804