5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose

Base Information

Chemical Name:5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose
CAS No.:88180-39-6
Molecular Formula:C₁₄H₁₄O₄
Molecular Weight:246.263
Hs Code.:

Synonyms:5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose

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Chemical Property of 5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose

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Technology Process of 5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose

There total 6 articles about 5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 88180-38-5
5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-arabino-hept-3-enose

: 88180-39-6
5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose

Guidance literature:: In diethyl ether; at 50 ℃;
DOI:10.1021/jo00177a026

Reference yield:

: 83938-00-5
((2R,3S,6S)-3-acetoxy-6-cyano-3,6-dihydro-2H-pyran-2-yl)methyl acetate

: 88180-39-6
5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose

Guidance literature:: Multi-step reaction with 4 steps

1: p-TsOH / methanol / 24 h / Ambient temperature

2: ZnCl₂ / 3 h

3: 85 percent / Diisobutylaluminum hydride / diethyl ether / 1 h / 0 °C

4: 85 percent / diethyl ether / 50 °C

With diisobutylaluminium hydride; toluene-4-sulfonic acid; zinc(II) chloride; In methanol; diethyl ether;
DOI:10.1021/jo00177a026

Reference yield:

: 88180-36-3
2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl cyanide

: 88180-39-6
5,7-O-Benzylidene-2,6-anhydro-3,4-dideoxy-aldehydo-D-erythro-hept-2-enose

Guidance literature:: Multi-step reaction with 3 steps

1: ZnCl₂ / 3 h

2: 85 percent / Diisobutylaluminum hydride / diethyl ether / 1 h / 0 °C

3: 85 percent / diethyl ether / 50 °C

With diisobutylaluminium hydride; zinc(II) chloride; In diethyl ether;
DOI:10.1021/jo00177a026