Carbamic acid, N-(5-bromo-4-methyl-2-thiazolyl)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, N-(5-bromo-4-methyl-2-thiazolyl)-, 1,1-dimethylethyl ester
CAS No.:947179-42-2
Molecular Formula:C₉H₁₃BrN₂O₂S
Molecular Weight:293.184
Hs Code.:2934100090
Mol file:947179-42-2.mol

Synonyms:Carbamic acid, N-(5-bromo-4-methyl-2-thiazolyl)-, 1,1-dimethylethyl ester

Suppliers and Price of Carbamic acid, N-(5-bromo-4-methyl-2-thiazolyl)-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(5-bromo-4-methylthiazol-2-yl)carbamate 95+%
5g
$ 671.00

Chemenu
tert-butyl(5-bromo-4-methylthiazol-2-yl)carbamate 95%
5g
$ 634.00

Chemcia Scientific
(5-Bromo-4-methyl-thiazol-2-yl)-carbamicacidtert-butylester ＞97%
1 G
$ 375.00

Alichem
tert-Butyl(5-bromo-4-methylthiazol-2-yl)carbamate
1g
$ 400.00

Total 5 raw suppliers

Chemical Property of Carbamic acid, N-(5-bromo-4-methyl-2-thiazolyl)-, 1,1-dimethylethyl ester

Chemical Property:

PKA:4.58±0.70(Predicted)
PSA：82.95000
Density:1.514±0.06 g/cm3(Predicted)
LogP:3.57460
Storage Temp.:2-8°C

Purity/Quality:

98% ^*data from raw suppliers

tert-Butyl(5-bromo-4-methylthiazol-2-yl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, N-(5-bromo-4-methyl-2-thiazolyl)-, 1,1-dimethylethyl ester

There total 2 articles about Carbamic acid, N-(5-bromo-4-methyl-2-thiazolyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3034-57-9
5-bromo-4-methyl-2-thiazolamine

: Boc₂O

: 947179-42-2
tert-butyl (5-bromo-4-methylthiazol-2-yl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;

Reference yield: 66.0%

: 3034-57-9
5-bromo-4-methyl-2-thiazolamine

: 24424-99-5
di-tert-butyl dicarbonate

: 947179-42-2
tert-butyl (5-bromo-4-methylthiazol-2-yl)carbamate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/j.bmcl.2013.04.077

Reference yield: 50.0%

: 947179-42-2
tert-butyl (5-bromo-4-methylthiazol-2-yl)carbamate

: 947179-43-3
tert-butyl (5-fluoro-4-methylthiazol-2-yl)carbamate

Guidance literature:: tert-butyl (5-bromo-4-methylthiazol-2-yl)carbamate; With n-butyllithium; In tetrahydrofuran; n-heptane; at -75 - -70 ℃; for 0.5h;

With N-fluorobis(benzenesulfon)imide; In tetrahydrofuran; n-heptane; at -78 - -75 ℃; for 2.58333h;

With ammonium chloride; In tetrahydrofuran; n-heptane; water;