C₂₄H₃₀F₃IOSi

Base Information

• Chemical Name: C₂₄H₃₀F₃IOSi
• CAS No.: 1369875-10-4
• Molecular Formula: C₂₄H₃₀F₃IOSi
• Molecular Weight: 546.487
• Mol file: 1369875-10-4.mol

Synonyms:C₂₄H₃₀F₃IOSi

Chemical Property of C₂₄H₃₀F₃IOSi

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₄H₃₀F₃IOSi

There total 2 articles about C₂₄H₃₀F₃IOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C8H12F3IO (1369875-09-1) + tert-butylchlorodiphenylsilane (58479-61-1) → C24H30F3IOSi (1369875-10-4)

Guidance literature:

With 1H-imidazole; In dichloromethane; at 25 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja211927b

Reference yield:

1-hydroxy-6-heptyne (63478-76-2) → C24H30F3IOSi (1369875-10-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dithionite; sodium hydrogencarbonate / water; acetonitrile / 0.67 h / 0 - 15 °C / Inert atmosphere

2: 1H-imidazole / dichloromethane / 2 h / 25 °C / Inert atmosphere

With 1H-imidazole; sodium dithionite; sodium hydrogencarbonate; In dichloromethane; water; acetonitrile;

DOI:10.1021/ja211927b

Reference yield: 92.0%

C24H30F3IOSi (1369875-10-4) → C24H29F3OSi (1369875-13-7)

Guidance literature:

With potassium tert-butylate; In benzene; at 25 ℃; for 5h; Inert atmosphere;

DOI:10.1021/ja211927b

upstream raw materials:

C₈H₁₂F₃IO

tert-butylchlorodiphenylsilane

1-hydroxy-6-heptyne

Downstream raw materials:

C₂₄H₂₉F₃OSi