C₃₄H₃₄N₈O₈S₂

Base Information

Chemical Name:C₃₄H₃₄N₈O₈S₂
CAS No.:1391396-78-3
Molecular Formula:C₃₄H₃₄N₈O₈S₂
Molecular Weight:746.825
Hs Code.:

C<sub>34</sub>H<sub>34</sub>N<sub>8</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₃₄H₃₄N₈O₈S₂

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Chemical Property of C₃₄H₃₄N₈O₈S₂

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Technology Process of C₃₄H₃₄N₈O₈S₂

There total 22 articles about C₃₄H₃₄N₈O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1399362-68-5
C₄₃H₅₀N₈O₁₀S₂

: 1391396-78-3
C₃₄H₃₄N₈O₈S₂

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1391396-36-3
C₂₇H₃₉N₃O₈

: 1391396-78-3
C₃₄H₃₄N₈O₈S₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

3.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

4.2: 12 h / -20 - 20 °C / Inert atmosphere

5.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

6.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

7.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

7.2: 3 h / 0 °C / Inert atmosphere

7.3: 3 h / 20 °C / Inert atmosphere

8.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

9.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

10.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

10.2: 3 h / 0 °C / Inert atmosphere

10.3: 3 h / 20 °C / Inert atmosphere

11.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

11.2: pH 1 / Acidic conditions

12.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

13.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

13.2: pH 1 / Acidic conditions

14.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 7.1: Hantzsch thiazole synthesis / 7.2: Hantzsch thiazole synthesis / 7.3: Hantzsch thiazole synthesis / 10.1: Hantzsch thiazole synthesis / 10.2: Hantzsch thiazole synthesis / 10.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: C₁₆H₂₆N₂O₆

: 1391396-78-3
C₃₄H₃₄N₈O₈S₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethanol

3.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

4.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

5.2: 12 h / -20 - 20 °C / Inert atmosphere

6.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

7.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

8.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

8.2: 3 h / 0 °C / Inert atmosphere

8.3: 3 h / 20 °C / Inert atmosphere

9.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

10.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

11.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

11.2: 3 h / 0 °C / Inert atmosphere

11.3: 3 h / 20 °C / Inert atmosphere

12.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

12.2: pH 1 / Acidic conditions

13.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

14.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

14.2: pH 1 / Acidic conditions

15.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 8.1: Hantzsch thiazole synthesis / 8.2: Hantzsch thiazole synthesis / 8.3: Hantzsch thiazole synthesis / 11.1: Hantzsch thiazole synthesis / 11.2: Hantzsch thiazole synthesis / 11.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105