C₃₃H₄₄O₈

Base Information

Chemical Name:C₃₃H₄₄O₈
CAS No.:391278-15-2
Molecular Formula:C₃₃H₄₄O₈
Molecular Weight:568.708
Hs Code.:

C<sub>33</sub>H<sub>44</sub>O<sub>8</sub>

Synonyms:C₃₃H₄₄O₈

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Chemical Property of C₃₃H₄₄O₈

Chemical Property:

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Technology Process of C₃₃H₄₄O₈

There total 17 articles about C₃₃H₄₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 391278-02-7
C₃₃H₄₂O₆

: 391278-15-2
C₃₃H₄₄O₈

Guidance literature:: With 4-methylmorpholine N-oxide; osmium(VIII) oxide;
DOI:10.1016/S0040-4039(01)01802-0

Reference yield:

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 391278-15-2
C₃₃H₄₄O₈

Guidance literature:: Multi-step reaction with 16 steps

1.1: 92 percent / EtAlCl₂ / toluene

2.1: 89 percent / H⁽¹⁺⁾

3.1: N-methylmorpholine-N-oxide / OsO₄

4.1: NaIO₄

5.1: 90 percent / m-chloroperbenzoic acid / CH₂Cl₂

6.1: 92 percent / H⁽¹⁺⁾

7.1: 100 percent / K₂CO₃ / methanol

8.1: 90 percent / pyridinium chlorochromate; 4 Angstroem MS / CH₂Cl₂

9.1: Et₃N

9.2: 89 percent / -78 °C

10.1: 73 percent / oxone / acetone

11.1: 79 percent / Al(Oi-Pr)3 / toluene

12.1: 96 percent / Et₃N

13.1: 100 percent / -78 °C

14.1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran

15.1: 86 percent / NaH / 80 °C

16.1: 85 percent / N-methylmorpholine-N-oxide / OsO₄

With Oxone; sodium periodate; 4 Angstroem MS; tetrabutyl ammonium fluoride; hydrogen cation; aluminum isopropoxide; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; osmium(VIII) oxide; ethylaluminum dichloride; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 1.1: Diels-Alder reaction / 5.1: Baeyer-Villiger oxidation / 11.1: Oppenauer ox. and Meerwein-Pondorf-Verley red.;
DOI:10.1016/S0040-4039(01)01802-0

Reference yield:

: 391278-09-4
6.8ac-Dimethyl-3c-isopropenyl-Δ⁶-(4arH)-octalon-(1)

: 391278-15-2
C₃₃H₄₄O₈

Guidance literature:: Multi-step reaction with 15 steps

1.1: 89 percent / H⁽¹⁺⁾

2.1: N-methylmorpholine-N-oxide / OsO₄

3.1: NaIO₄

4.1: 90 percent / m-chloroperbenzoic acid / CH₂Cl₂

5.1: 92 percent / H⁽¹⁺⁾

6.1: 100 percent / K₂CO₃ / methanol

7.1: 90 percent / pyridinium chlorochromate; 4 Angstroem MS / CH₂Cl₂

8.1: Et₃N

8.2: 89 percent / -78 °C

9.1: 73 percent / oxone / acetone

10.1: 79 percent / Al(Oi-Pr)3 / toluene

11.1: 96 percent / Et₃N

12.1: 100 percent / -78 °C

13.1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran

14.1: 86 percent / NaH / 80 °C

15.1: 85 percent / N-methylmorpholine-N-oxide / OsO₄

With Oxone; sodium periodate; 4 Angstroem MS; tetrabutyl ammonium fluoride; hydrogen cation; aluminum isopropoxide; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; osmium(VIII) oxide; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 4.1: Baeyer-Villiger oxidation / 10.1: Oppenauer ox. and Meerwein-Pondorf-Verley red.;
DOI:10.1016/S0040-4039(01)01802-0