C₄₁H₄₄N₂O₇Si

Base Information

Chemical Name:C₄₁H₄₄N₂O₇Si
CAS No.:1093849-14-9
Molecular Formula:C₄₁H₄₄N₂O₇Si
Molecular Weight:704.895
Hs Code.:

C<sub>41</sub>H<sub>44</sub>N<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₄₁H₄₄N₂O₇Si

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Chemical Property of C₄₁H₄₄N₂O₇Si

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Technology Process of C₄₁H₄₄N₂O₇Si

There total 13 articles about C₄₁H₄₄N₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093849-13-8
C₃₉H₄₄O₇Si

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 1093849-14-9
C₄₁H₄₄N₂O₇Si

Guidance literature:: C₃₉H₄₄O₇Si; uracil; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 40 ℃; for 0.25h;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 70 ℃; for 4h;

Reference yield:

: 939-26-4
2-bromomethylnaphthyl bromide

: 1093849-14-9
C₄₁H₄₄N₂O₇Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

1.2: 2 h

2.1: acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane / 1.5 h / 20 °C

4.1: sodium hydroxide / water; tetrahydrofuran / 48 h / 20 °C / Cooling with ice

5.1: triethylamine / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 0.25 h / -78 °C

7.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / Cooling with ice

7.2: 1.5 h / -78 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: 0.25 h / -78 °C

9.1: cerium(III) chloride / tetrahydrofuran / 1.75 h / Cooling with ice

9.2: 1.5 h / -78 °C

10.1: thionyl chloride; pyridine / 1 h / 60 °C

11.1: sulfuric acid / water / 1 h / 20 °C

12.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

12.2: 4 h / 0 - 70 °C

With pyridine; sodium periodate; thionyl chloride; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; sulfuric acid; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 6.1: Swern Oxidation / 6.2: Swern Oxidation / 8.1: Swern Oxidation / 8.2: Swern Oxidation;

Reference yield:

: 1091607-89-4
(R)-1-((3aR,5R,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 1093849-14-9
C₄₁H₄₄N₂O₇Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium periodate / 1,4-dioxane / 1.5 h / 20 °C

2.1: sodium hydroxide / water; tetrahydrofuran / 48 h / 20 °C / Cooling with ice

3.1: triethylamine / 16 h / 0 - 20 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

4.2: 0.25 h / -78 °C

5.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / Cooling with ice

5.2: 1.5 h / -78 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 0.25 h / -78 °C

7.1: cerium(III) chloride / tetrahydrofuran / 1.75 h / Cooling with ice

7.2: 1.5 h / -78 °C

8.1: thionyl chloride; pyridine / 1 h / 60 °C

9.1: sulfuric acid / water / 1 h / 20 °C

10.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

10.2: 4 h / 0 - 70 °C

With pyridine; sodium periodate; thionyl chloride; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; sulfuric acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile; 4.1: Swern Oxidation / 4.2: Swern Oxidation / 6.1: Swern Oxidation / 6.2: Swern Oxidation;