tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate

Base Information

• Chemical Name: tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate
• CAS No.: 1217317-65-1
• Molecular Formula: C₁₉H₃₀N₂O₄
• Molecular Weight: 350.458

Synonyms:tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate

Chemical Property of tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate

Chemical Property:

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Technology Process of tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate

There total 2 articles about tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + benzyl N-[1-(aminomethyl)-3-methyl-butyl]carbamate (228557-26-4) → tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate (1217317-65-1)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1021/cc1000105

Reference yield:

→ tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate (1217317-65-1)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; for 16h; Inert atmosphere;

With water; In tetrahydrofuran; for 6h;

Reference yield: 28.0%

tert-butyl N-[(2S)-2-(benzyloxycarbonylamino)-4-methyl-pentyl]carbamate (1217317-65-1) → tert-butyl N-[(2S)-2-amino-4-methylpentyl]carbamate (1217317-66-2)

Guidance literature:

With 5% Pd(II)/C(eggshell); hydrogen; In methanol; for 18h;

DOI:10.1021/cc1000105

upstream raw materials:

di-tert-butyl dicarbonate

benzyl N-[1-(aminomethyl)-3-methyl-butyl]carbamate

Downstream raw materials:

tert-butyl N-[(2S)-2-amino-4-methylpentyl]carbamate

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