Technology Process of C55H59N3Si
There total 4 articles about C55H59N3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetra-n-butylammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 20 °C
2: 73 mg / Et3N / Pd(PPh3)4; CuI / 2 h / Heating
With
tetrabutyl ammonium fluoride; acetic acid; triethylamine;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
DOI:10.1021/jo050833d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3.19 g / Et3N / PdCl2(PPh3)2; CuI / 3 h / 20 °C
2: tetra-n-butylammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 20 °C
3: 73 mg / Et3N / Pd(PPh3)4; CuI / 2 h / Heating
With
tetrabutyl ammonium fluoride; acetic acid; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
DOI:10.1021/jo050833d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: K2CO3; MeOH / tetrahydrofuran / 1 h / 20 °C
2: 3.19 g / Et3N / PdCl2(PPh3)2; CuI / 3 h / 20 °C
3: tetra-n-butylammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 20 °C
4: 73 mg / Et3N / Pd(PPh3)4; CuI / 2 h / Heating
With
methanol; tetrabutyl ammonium fluoride; potassium carbonate; acetic acid; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
DOI:10.1021/jo050833d
