6-cyclohexyl-2,8-dimethylphenanthridine

Base Information

• Chemical Name: 6-cyclohexyl-2,8-dimethylphenanthridine
• CAS No.: 1613289-95-4
• Molecular Formula: C₂₁H₂₃N
• Molecular Weight: 289.42
• Mol file: 1613289-95-4.mol

Synonyms:6-cyclohexyl-2,8-dimethylphenanthridine

Chemical Property of 6-cyclohexyl-2,8-dimethylphenanthridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 6-cyclohexyl-2,8-dimethylphenanthridine

There total 3 articles about 6-cyclohexyl-2,8-dimethylphenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

cyclohexane (110-82-7,25012-93-5) + 2-isocyano-4’,5-dimethyl-1,1’-biphenyl → 6-cyclohexyl-2,8-dimethylphenanthridine (1613289-95-4)

Guidance literature:

With copper(I) oxide; di-tert-butyl peroxide; at 120 ℃; for 24h; Reagent/catalyst; Temperature; Sealed tube;

DOI:10.1039/c4ob01256a

Reference yield: 65.0%

1-bromocyclohexane (108-85-0) + 2-isocyano-4’,5-dimethyl-1,1’-biphenyl → 6-cyclohexyl-2,8-dimethylphenanthridine (1613289-95-4)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; {Au(dppm)}2Cl₂; sodium carbonate; In acetonitrile; for 16h; Sealed tube; Inert atmosphere; UV-irradiation;

DOI:10.1021/acs.joc.8b01380

Reference yield: 50.0%

cyclohexane (110-82-7,25012-93-5) + C15H13N (1465674-22-9) → 6-cyclohexyl-2,8-dimethylphenanthridine (1613289-95-4)

Guidance literature:

With copper (II)-fluoride; bis(1-methyl-1-phenylethyl)peroxide; at 110 ℃; for 7h; Sealed tube;

DOI:10.1021/ol501461u

upstream raw materials:

cyclohexane

C₁₅H₁₃N

1-bromocyclohexane