(2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine

Base Information

Chemical Name:(2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine
CAS No.:132910-87-3
Molecular Formula:C₃₈H₅₈Cl₃NO₃Si
Molecular Weight:711.328
Hs Code.:

Synonyms:(2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine

Chemical Property:

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Technology Process of (2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine

There total 4 articles about (2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142921-04-8
N-[(E)-(1S,2R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-trityloxymethyl-nonadec-3-enyl]-2,2,2-trichloro-acetamide

: 132910-87-3
(2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 2h; Yield given; Ambient temperature;

Reference yield:

: 6918-49-6
<2(S),3(R),4E>-2-amino-4-eicosene-1,3-diol

: 132910-87-3
(2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine

Guidance literature:: Multi-step reaction with 4 steps

1: 1) pyridine 2) NaOMe / 1) CH₂Cl₂, 15 h, r.t. 2) THF, MeOH, 30 min, r.t.

2: 86 percent / pyridine / CH₂Cl₂ / 19 h / Heating

3: imidazole / dimethylformamide / 44 h / 100 °C

4: p-TsOH*H₂O / methanol / 2 h / Ambient temperature

With pyridine; 1H-imidazole; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 132910-85-1
(2S,3R,4E)-N-Trichloroacetyl-4-icosasphingenine

: 132910-87-3
(2S,3R,4E)-N-Trichloroacetyl-3-O-(tert-butyldiphenylsilyl)-4-icosasphingosine

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / pyridine / CH₂Cl₂ / 19 h / Heating

2: imidazole / dimethylformamide / 44 h / 100 °C

3: p-TsOH*H₂O / methanol / 2 h / Ambient temperature

With pyridine; 1H-imidazole; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;