tetrabutylammonium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]bis[3,5-bis(trifluoromethyl)phenyl]borate

Base Information

Chemical Name:tetrabutylammonium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]bis[3,5-bis(trifluoromethyl)phenyl]borate
CAS No.:1013095-33-4
Molecular Formula:C₁₆H₃₆N*C₄₂H₄₀BF₂₀O₂Si₂
Molecular Weight:1266.2
Hs Code.:

Synonyms:tetrabutylammonium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]bis[3,5-bis(trifluoromethyl)phenyl]borate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrabutylammonium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]bis[3,5-bis(trifluoromethyl)phenyl]borate

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Technology Process of tetrabutylammonium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]bis[3,5-bis(trifluoromethyl)phenyl]borate

There total 2 articles about tetrabutylammonium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]bis[3,5-bis(trifluoromethyl)phenyl]borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1013095-29-8
potassium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]difluoroborate

: 328-70-1
3,6-bis(trifluoromethyl)bromobenzene

: 1643-19-2
tetrabutylammomium bromide

: 1013095-33-4
tetrabutylammonium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]bis[3,5-bis(trifluoromethyl)phenyl]borate

Guidance literature:: potassium bis[4-(tert-butyldimethylsilanyloxymethyl)-2,3,5,6-tetrafluorophenyl]difluoroborate; 3,6-bis(trifluoromethyl)bromobenzene; With isopropylmagnesium chloride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 135h;

tetrabutylammomium bromide; In dichloromethane; at 20 ℃; for 0.5h; Further stages.;
DOI:10.1055/s-2007-1000862