N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline

Base Information

• Chemical Name: N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline
• CAS No.: 215527-65-4
• Molecular Formula: C₂₈H₁₉Cl₂N₃S
• Molecular Weight: 500.451
• Mol file: 215527-65-4.mol

Synonyms:N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline

Chemical Property of N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline

There total 2 articles about N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2,4-dichlorobenzenesulfenyl chloride (38064-02-7) + 4-phenyl-2,6-di(3-pyridyl)aniline (215527-63-2) → N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline (215527-65-4)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 2h;

DOI:10.1021/jo981155g

Reference yield:

2,4-dichlorobenzenethiol (1122-41-4) → N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline (215527-65-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Cl₂ / CH₂Cl₂

2: 74 percent / Et₃N / tetrahydrofuran / 2 h / 0 °C

With chlorine; triethylamine; In tetrahydrofuran; dichloromethane; 1: Chlorination / 2: Substitution;

DOI:10.1021/jo981155g

Reference yield: 31.0%

N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)aniline (215527-65-4) → N-[(2,4-dichlorophenyl)thio]-4-phenyl-2,6-di(3-pyridyl)phenylaminyl

Guidance literature:

With potassium carbonate; lead dioxide; In benzene; for 0.05h;

DOI:10.1021/jo981155g

upstream raw materials:

2,4-dichlorobenzenesulfenyl chloride

4-phenyl-2,6-di(3-pyridyl)aniline

2,4-dichlorobenzenethiol