9-(4-Methylphenyl)-9H-fluorene

Base Information

• Chemical Name: 9-(4-Methylphenyl)-9H-fluorene
• CAS No.: 18153-43-0
• Molecular Formula: C20H16
• Molecular Weight: 256.347
• NSC Number: 86495
• DSSTox Substance ID: DTXSID00171163
• Nikkaji Number: J1.557.282E
• Wikidata: Q83041255
• Mol file: 18153-43-0.mol

Synonyms:9-(4-METHYLPHENYL)-9H-FLUORENE;18153-43-0;9-(p-methylphenyl)fluorene;NSC86495;9-p-Tolyl-fluorene;DTXSID00171163;NSC 86495;NSC-86495

Chemical Property of 9-(4-Methylphenyl)-9H-fluorene

Chemical Property:

• Vapor Pressure: 4.09E-06mmHg at 25°C
• Boiling Point: 395.8°C at 760 mmHg
• Flash Point: 186.9°C
• Density: 1.12g/cm³
• XLogP3: 5.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 256.125200510
• Heavy Atom Count: 20
• Complexity: 303

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)C2C3=CC=CC=C3C4=CC=CC=C24

Technology Process of 9-(4-Methylphenyl)-9H-fluorene

There total 16 articles about 9-(4-Methylphenyl)-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

acetic acid (biphenyl-2-yl)(p-tolyl)methyl ester (1065544-22-0) → 9-(4-methylphenyl)fluorene (18153-43-0)

Guidance literature:

With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 0.0166667h;

DOI:10.1016/j.tet.2008.07.021

Reference yield: 96.0%

9H-fluorene (86-73-7) + para-chlorotoluene (106-43-4) → 9-(4-methylphenyl)fluorene (18153-43-0)

Guidance literature:

With NHC-Pd(II)-Im; potassium tert-butylate; In 1,4-dioxane; at 120 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c4ob01594k

Reference yield: 95.0%

(biphenyl-2-yl)(p-tolyl)methanol (1065543-98-7) → 9-(4-methylphenyl)fluorene (18153-43-0)

Guidance literature:

With iron(III) chloride; In nitromethane; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.tetlet.2012.08.005

upstream raw materials:

9-(4-methylphenyl)-9H-fluoren-9-ol

9-Phenyl-9-p-tolyl-9H-fluorene

9-Fluorenol

toluene

Downstream raw materials:

(C₅H₅)ZrCl₂(C₁₃H₈C₆H₄CH₃)

9-Benzhydryl-9-p-tolyl-9H-fluorene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 18153-43-0 9-(4-methylphenyl)-9H-fluorene

Send

Send

Metric Ton KG G Pound L ML

Send

Send