methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate

Base Information

Chemical Name:methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate
CAS No.:350818-09-6
Molecular Formula:C₁₇H₂₀F₃NO₄S
Molecular Weight:391.411
Hs Code.:

Synonyms:methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate

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Chemical Property of methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate

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Technology Process of methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate

There total 1 articles about methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1192-37-6
methylenecyclohexane

: 2-[(E)-Benzenesulfonylimino]-3,3,3-trifluoro-propionic acid methyl ester

: 350818-09-6
methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1055/s-2001-13362

Reference yield:

: 350818-09-6
methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate

: 1-benzenesulfonyl-4-hex-5-enyl-2-trifluoromethyl-1,2,3,6-tetrahydro-pyridine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.5 h / 0 °C

1.2: dimethylformamide / 2 h / 20 °C

2.1: 74 percent / Grubbs' catalyst / CH₂Cl₂ / 20 °C

With sodium hydride; Grubbs catalyst first generation; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2001-13362

Reference yield:

: 106-95-6
allyl bromide

: 350818-09-6
methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate

: 350818-15-4
2-(allyl-benzenesulfonyl-amino)-2-cyclohex-1-enylmethyl-3,3,3-trifluoro-propionic acid methyl ester

Guidance literature:: methyl 3-(cyclohex-1-enyl)-2-phenylsulfonylamino-2-trifluoromethylpropionate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

allyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1055/s-2001-13362