Technology Process of (E)-8-phenyloct-5-en-2-one
There total 11 articles about (E)-8-phenyloct-5-en-2-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium dihydrogenphosphate; sodium amalgam;
In
tetrahydrofuran; methanol;
at -30 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/ja207944c
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h / Inert atmosphere
1.2: Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
3.1: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux
4.1: sodium amalgam; potassium dihydrogenphosphate / tetrahydrofuran; methanol / 4 h / -30 °C / Inert atmosphere
With
potassium dihydrogenphosphate; sodium amalgam; dilauryl peroxide; sodium hydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; mineral oil;
DOI:10.1021/ja207944c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
2: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux
3: sodium amalgam; potassium dihydrogenphosphate / tetrahydrofuran; methanol / 4 h / -30 °C / Inert atmosphere
With
potassium dihydrogenphosphate; sodium amalgam; dilauryl peroxide; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja207944c
