allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

Base Information

• Chemical Name: allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate
• CAS No.: 524071-53-2
• Molecular Formula: C₃₇H₃₇N₂O₅P
• Molecular Weight: 620.685

Synonyms:allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

Chemical Property of allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

Chemical Property:

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Technology Process of allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

There total 1 articles about allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyl [(2R,3S)-2-[2-(4-{[(tert-butoxycarbonyl)-amino]-methyl}-phenyl)-2-oxoethyl]-3-((1R)-1-{[tert-butyl-(dimethyl)-silyl]-oxy}-ethyl)-4-oxoazetidin-1-yl] (triphenylphosphoranilidene) acetate (524071-52-1) → allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate (524071-53-2)

Guidance literature:

With trifluoroacetic acid; In water;

Reference yield:

allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate (524071-53-2) + pyridine-3-carbonyl chloride hydrochloride (20260-53-1) → allyl {(3S,4R)-3-[(1R)-1-hydroxyethyl]-2-oxo-4-[2-oxo-2-(4-{[(pyridin-3-ylcarbonyl)-amino]-methyl}-phenyl)-ethyl]-azetidin-1-yl} (triphenylphosphoranilidene) acetate (524072-69-3)

Guidance literature:

With pyridine; triethylamine; In tetrahydrofuran; at 20 ℃; for 0.166667h;

Reference yield:

allyl {(2R,3S)-2-{2-[4-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate (524071-53-2) + (5-methyl-2-oxo-1,3-dioxol-4-yl)methyl 4-nitrophenyl carbonate (173604-87-0) → allyl [(2R,3S)-3-[(1R)-1-hydroxyethyl]-2-(2-{4-[({[(5-methyl-2-oxo-1,3-dioxol-4-yl)-methoxy]-carbonyl}-amino)-methyl]-phenyl}-2-oxoethyl)-4-oxoazetidin-1-yl] (triphenylphosphoranilidene) acetate (524071-84-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 36h;

upstream raw materials:

allyl [(2R,3S)-2-[2-(4-{[(tert-butoxycarbonyl)-amino]-methyl}-phenyl)-2-oxoethyl]-3-((1R)-1-{[tert-butyl-(dimethyl)-silyl]-oxy}-ethyl)-4-oxoazetidin-1-yl] (triphenylphosphoranilidene) acetate

Downstream raw materials:

allyl {(2R,3S)-2-[2-(4-{[(aminocarbonyl)-amino]-methyl}-phenyl)-2-oxoethyl]-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

allyl {(3S,4R)-3-[(1R)-1-hydroxyethyl]-2-oxo-4-[2-oxo-2-(4-{[(pyridin-3-ylcarbonyl)-amino]-methyl}-phenyl)-ethyl]-azetidin-1-yl} (triphenylphosphoranilidene) acetate

allyl [(2R,3S)-3-[(1R)-1-hydroxyethyl]-2-(2-{4-[({[(5-methyl-2-oxo-1,3-dioxol-4-yl)-methoxy]-carbonyl}-amino)-methyl]-phenyl}-2-oxoethyl)-4-oxoazetidin-1-yl] (triphenylphosphoranilidene) acetate

allyl ((2R,3S)-2-{2-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-2-oxoethyl}-4-oxo-3-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-azetidin-1-yl) (triphenylphosphoranilidene) acetate

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