p-toluenebenzenesulfonyl azide-¹⁵N

Base Information

Chemical Name:p-toluenebenzenesulfonyl azide-¹⁵N
CAS No.:1609375-70-3
Molecular Formula:C₇H₇N₃O₂S
Molecular Weight:198.211
Hs Code.:

p-toluenebenzenesulfonyl azide-<SUP>15</SUP>N

Synonyms:p-toluenebenzenesulfonyl azide-¹⁵N

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-toluenebenzenesulfonyl azide-¹⁵N

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Technology Process of p-toluenebenzenesulfonyl azide-¹⁵N

There total 2 articles about p-toluenebenzenesulfonyl azide-¹⁵N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 287476-18-0
4-methyl[¹⁵N]benzene-1-sulfonamide

: 1609375-70-3
p-toluenebenzenesulfonyl azide-¹⁵N

Guidance literature:: With 3-azidosulfonyl-3H-imidazole-1-ium hydrogen sulfate; potassium carbonate; In water; isopropyl alcohol; at 20 ℃; for 18h;
DOI:10.1021/jo500553q

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1609375-70-3
p-toluenebenzenesulfonyl azide-¹⁵N

: tosyl azide

Guidance literature:: With Na⁽¹⁺⁾*⁽¹⁵⁾NN₂^(1-)=Na⁽¹⁵⁾NN₂; In water; acetone; at 0 - 20 ℃; for 18h; Overall yield = 93 percent;
DOI:10.1002/anie.202002750