methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate

Base Information

Chemical Name:methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate
CAS No.:67201-24-5
Molecular Formula:C₁₅H₃₀O₃Si₂
Molecular Weight:314.572
Hs Code.:

Synonyms:methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate

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Technology Process of methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate

There total 6 articles about methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 80400-53-9
(E)-1-trimethylsilyl-3-trimethylsilyloxybuta-1,3-diene

: 80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7
methacrylic acid methyl ester

: 67201-24-5
methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate

Guidance literature:: With hydroquinone; at 130 ℃; for 64h;
DOI:10.1039/P19810002415

Reference yield:

: 49750-09-6
(E)-1-trimethylsilyl-1-buten-3-one

: 67201-24-5
methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / BuLi, di-isopropylamine / tetrahydrofuran; hexane / 4 h / -78 - 20 °C

2: 46 percent / hydroquinone / 64 h / 130 °C

With n-butyllithium; diisopropylamine; hydroquinone; In tetrahydrofuran; hexane;
DOI:10.1039/P19810002415

Reference yield:

: 56919-90-5
(E)-4-(trimethylsilyl)but-3-en-2-ol

: 67201-24-5
methyl 1-methyl-2-trimethylsilyl-4-trimethylsilyloxycyclohex-3-enecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / manganese dioxide / light petroleum / 12 h / Ambient temperature

2: 84 percent / BuLi, di-isopropylamine / tetrahydrofuran; hexane / 4 h / -78 - 20 °C

3: 46 percent / hydroquinone / 64 h / 130 °C

With manganese(IV) oxide; n-butyllithium; diisopropylamine; hydroquinone; In tetrahydrofuran; hexane; Petroleum ether;
DOI:10.1039/P19810002415