N-<1-(N¹,N¹-Dimethyl-N²-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid

Base Information

• Chemical Name: N-<1-(N¹,N¹-Dimethyl-N²-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid
• CAS No.: 77767-47-6
• Molecular Formula: C₁₇H₂₆N₄O₂S
• Molecular Weight: 350.485

Synonyms:N-<1-(N¹,N¹-Dimethyl-N²-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid

Chemical Property of N-<1-(N¹,N¹-Dimethyl-N²-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid

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Technology Process of N-<1-(N¹,N¹-Dimethyl-N²-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid

There total 1 articles about N-<1-(N¹,N¹-Dimethyl-N²-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

Isopropyl(tosyl)carbodiimid (19978-10-0) + 3-dimethylamino-2,2-dimethyl-2H-azirine (54856-83-6) → N-<1-(N1,N1-Dimethyl-N2-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid (77767-47-6) + N2-(N1-Isopropyl-N2-tosylamidino)-N1,N1-dimethylmethacrylamidin (77767-48-7) + 1-<α-(N2-Benzyl-N1,N1-dimethylamidino)isopropyl>-3-isopropyl-2-tosylguanidin (77767-49-8) + N-(4-Dimethylimonio-3-isopropyl-5,5-dimethyl-1-imidazolin-2-yl)tosylamidat (77767-41-0)

Guidance literature:

In diethyl ether; Ambient temperature;

Reference yield: 22.0%

N-<1-(N1,N1-Dimethyl-N2-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid (77767-47-6) → N,N,4-trimethylbenzenesulfonamide (599-69-9) + 3-Isopropyl-5,5-dimethyl-2-tosylimino-4-imidazolidinon (77767-50-1)

Guidance literature:

With water; acetone; for 24h; Ambient temperature;

Reference yield: 21.0%

N-<1-(N1,N1-Dimethyl-N2-tosylamidino)-1-methylethyl>-N'-isopropylcarbodiimid (77767-47-6) + benzylamine (100-46-9) → N,N,4-trimethylbenzenesulfonamide (599-69-9) + 4-Benzylimino-3-isopropyl-5,5-dimethyl-2-(tosylimino)imidazolidin (77767-82-9)

Guidance literature:

In dichloromethane; for 48h; Ambient temperature;

upstream raw materials:

Isopropyl(tosyl)carbodiimid

3-dimethylamino-2,2-dimethyl-2H-azirine

Downstream raw materials:

N,N,4-trimethylbenzenesulfonamide

3-Isopropyl-5,5-dimethyl-2-tosylimino-4-imidazolidinon

4-Benzylimino-3-isopropyl-5,5-dimethyl-2-(tosylimino)imidazolidin

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