C₂₉H₄₄O₄Si

Base Information

• Chemical Name: C₂₉H₄₄O₄Si
• CAS No.: 1443743-44-9
• Molecular Formula: C₂₉H₄₄O₄Si
• Molecular Weight: 484.751
• Mol file: 1443743-44-9.mol

Synonyms:C₂₉H₄₄O₄Si

Chemical Property of C₂₉H₄₄O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₉H₄₄O₄Si

There total 1 articles about C₂₉H₄₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C39H61O9PSi (1443743-45-0) → C29H44O4Si (1443743-44-9) + C58H88O8Si2

Guidance literature:

C₃₉H₆₁O₉PSi; With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile; at 20 ℃; for 12h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In aq. phosphate buffer; dichloromethane; at 0 ℃; for 0.1h; pH=7.5; Inert atmosphere; Darkness;

With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.1h; Inert atmosphere;

DOI:10.1021/ol401367h

Reference yield:

C29H44O4Si (1443743-44-9) → C29H46O4Si

Guidance literature:

With L-Selectride; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ol401367h

Reference yield:

C29H44O4Si (1443743-44-9) → C31H52O5Si2

Guidance literature:

Multi-step reaction with 4 steps

1.1: L-Selectride / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 0.01 h / -10 °C / Inert atmosphere

3.1: ozone; pyridine / dichloromethane / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: potassium carbonate / methanol / 0.6 h / 20 °C

With pyridine; 2,6-dimethylpyridine; L-Selectride; potassium carbonate; ozone; In tetrahydrofuran; methanol; dichloromethane; 1.1: |Aldol Addition / 4.1: |Aldol Addition;

DOI:10.1021/ol401367h

upstream raw materials:

C₃₉H₆₁O₉PSi

Downstream raw materials:

C₃₂H₅₄O₄Si₂

C₃₁H₅₂O₅Si₂