5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole
CAS No.:233750-76-0
Molecular Formula:C₁₇H₂₂N₄S
Molecular Weight:314.454
Hs Code.:

Synonyms:5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole

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Technology Process of 5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole

There total 5 articles about 5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 233750-63-5
(S,3Z,6E)-3,5-dimethylocta-3,6-dien-1-ol

: 233750-76-0
5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1021/ja9904686

Reference yield:

: 161912-62-5
(3R,4S,5E)-3-hydroxy-2,4-dimethylhepta-1,5-diene

: 233750-76-0
5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / Sharpless reagent, D-DET

2: 96 percent / imidazole

3: 1.) CuI, 2.) K₂CO₃ / 1.) THF, from -50 deg C to RT, 2.) MeOH

4: 1.) Me₂NCH(OMe)2, 2.) Ac₂O, 3.) KH, tBuOOH, CsF, NMP

5: 82 percent / DIAD_. Ph₃P / dimethylformamide

With 1H-imidazole; 1-methyl-pyrrolidin-2-one; tert.-butylhydroperoxide; copper(l) iodide; diethyl (2S,3S)-tartrate; di-isopropyl azodicarboxylate; Sharpless reagent; acetic anhydride; potassium hydride; potassium carbonate; N,N-dimethyl-formamide dimethyl acetal; triphenylphosphine; cesium fluoride; In N,N-dimethyl-formamide;
DOI:10.1021/ja9904686

Reference yield:

: 233750-72-6
(E)-(1R,2S)-2-Methyl-1-((S)-2-methyl-oxiranyl)-pent-3-en-1-ol

: 233750-76-0
5-((3Z,6E)-(S)-3,5-Dimethyl-octa-3,6-dienylsulfanyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / imidazole

2: 1.) CuI, 2.) K₂CO₃ / 1.) THF, from -50 deg C to RT, 2.) MeOH

3: 1.) Me₂NCH(OMe)2, 2.) Ac₂O, 3.) KH, tBuOOH, CsF, NMP

4: 82 percent / DIAD_. Ph₃P / dimethylformamide

With 1H-imidazole; 1-methyl-pyrrolidin-2-one; tert.-butylhydroperoxide; copper(l) iodide; di-isopropyl azodicarboxylate; acetic anhydride; potassium hydride; potassium carbonate; N,N-dimethyl-formamide dimethyl acetal; triphenylphosphine; cesium fluoride; In N,N-dimethyl-formamide;
DOI:10.1021/ja9904686