2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate

Base Information

Chemical Name:2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate
CAS No.:1432413-22-3
Molecular Formula:C₁₄H₂₀N₆O₄S
Molecular Weight:368.417
Hs Code.:

Synonyms:2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate

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Chemical Property of 2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate

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Technology Process of 2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate

There total 2 articles about 2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1432576-80-1
2-((4-((1H-1,2,4-triazol-3-yl)diazenyl)phenyl)(ethyl)amino)ethyl sulfate, sodium salt

: 80-48-8
methyl p-toluene sulfonate

: 1432413-22-3
2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate

Guidance literature:: at 90 ℃; for 5h;

Reference yield:

: 92-50-2
2-( N-ethylanilino)ethanol

: 1432413-22-3
2-[{4-[(1,4-dimethyl-4H-1,2,4-triazol-1-ium-5-yl)diazenyl]phenyl}(ethyl)amino]ethyl sulfate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / ethanol / 2 h / 35 - 40 °C

2.1: nitrosylsulfuric acid; sulfuric acid; acetic acid / water / 2 h / 0 - 5 °C

2.2: 10 - 20 °C

2.3: pH 7

3.1: 5 h / 90 °C

With nitrosylsulfuric acid; sulfuric acid; acetic acid; In ethanol; water;