4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide

Base Information

Chemical Name:4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide
CAS No.:305818-61-5
Molecular Formula:C₂₁H₂₇Br₂N₃O₂P₂S
Molecular Weight:607.286
Hs Code.:

Synonyms:4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide

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Chemical Property of 4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide

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Technology Process of 4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide

There total 3 articles about 4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 216017-08-2
4-(N,N-methylphenylamino)phenylphosphonothioic dimorpholide

: 305818-61-5
4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide

Guidance literature:: With pyridine; phosphorus tribromide; Heating;

Reference yield:

: 552-82-9
benzhydrylidene(methyl)amine

: 305818-61-5
4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 74 percent / PBr₃; pyridine / 8 h / 20 °C

2.1: Et₃N / benzene / 1 h

2.2: 67 percent / sulfur / benzene / 2 h / Heating

3.1: 56 percent / PBr₃; pyridine / Heating

With pyridine; phosphorus tribromide; triethylamine; In benzene;

Reference yield:

: 216017-05-9
4-(N,N-methylphenylamino)phenyldibromophosphine

: 305818-61-5
4-[N-(4-Dibromophosphinophenyl)-N-methylamino]phenylphosphinothioic dimorpholide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / benzene / 1 h

1.2: 67 percent / sulfur / benzene / 2 h / Heating

2.1: 56 percent / PBr₃; pyridine / Heating

With pyridine; phosphorus tribromide; triethylamine; In benzene;