1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate

Base Information

Chemical Name:1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate
CAS No.:1266342-67-9
Molecular Formula:C₂₃H₃₀O₇S₂
Molecular Weight:482.619
Hs Code.:

Synonyms:1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate

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Technology Process of 1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate

There total 1 articles about 1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1266342-27-1
3-phenoxysulfonyl-1-propanesulfonyl chloride

: 147252-93-5
(3S)-3-(benzyloxy)-2,2-dimethyl-4-penten-1-ol

: 1266342-67-9
1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 18h;

Reference yield: 100.0%

: 1266342-67-9
1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate

: 1266342-69-1
1-[(3R)-3-benzyloxy-2,2-dimethyl-4-oxo-butyl]-phenyl propane-1,3-disulfonate

Guidance literature:: With dimethylsulfide; ozone; In dichloromethane; at -78 - 20 ℃;

Reference yield:

: 1266342-67-9
1-[(3S)-3-benzyloxy-2,2-dimethyl-pent-4-enyl]-phenyl propane-1,3-disulfonate

: 1266343-12-7
ethyl (2R)-2-benzyloxy-3,3-dimethyl-4-(3-phenoxysulfonylpropylsulfonyloxy)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: ozone; dimethylsulfide / dichloromethane / -78 - 20 °C

2: chromium(VI) oxide; sulfuric acid / water; acetone / 1 h / 0 °C

3: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h

With chromium(VI) oxide; oxalyl dichloride; dimethylsulfide; sulfuric acid; ozone; N,N-dimethyl-formamide; In dichloromethane; water; acetone;