(2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol

Base Information

Chemical Name:(2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol
CAS No.:207915-72-8
Molecular Formula:C₁₉H₂₈O
Molecular Weight:272.431
Hs Code.:

Synonyms:(2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol

Chemical Property:

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Technology Process of (2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol

There total 1 articles about (2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41891-54-7
diethyl 3-(ethoxycarbonyl)-3-methylprop-2-en-yl phosphate

: 28075-36-7
2,6-dimethyl-1-cyclohexen-1-yl triflate

: 207915-64-8
(2E,4E)-3-methyl-5-(tributylstannyl)-2,4-pentadien-1-al

: 207915-72-8
(2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1021/jo980097w

Reference yield: 47.0%

: 207915-72-8
(2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol

: 52152-27-9
1-demethylretinal

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; In dichloromethane; 1.) 0 deg C, 1 h, 2.) room temperature, 1 h;
DOI:10.1021/jo980097w

Reference yield:

: 207915-72-8
(2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-ol

: (2E,4E,6E,8E)-9-(2,6-Dimethyl-cyclohex-1-enyl)-3,7-dimethyl-nona-2,4,6,8-tetraenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / 4A MS, NMO, TPAP / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2.) room temperature, 1 h

2: 72 percent / KCN, MnO₂ / 2 h / 0 °C

3: 78 percent / aq. KOH / ethanol / 0.17 h / Heating

With potassium cyanide; manganese(IV) oxide; potassium hydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; In ethanol; dichloromethane;
DOI:10.1021/jo980097w